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001-es BibID:	BIBFORM135986
035-os BibID:	(wos)001652152100006
Első szerző:	Farsang Róbert
Cím:	Nitrite and Nitrate Analysis by Capillary Electrophoresis with Direct UV Absorbance Detection : a Mini-Review / Farsang Róbert, Hogyor Kinga, Járvás Gábor, Guttman András
Dátum:	2025
ISSN:	0133-0276
Megjegyzések:	The analysis of nitrite and nitrate ions is of great importance in environmental samples, food and various human samples. In contrast to conventional spectrophotometric methods, nitrite and nitrate ions are relatively easy to analyze by capillary electrophoresis as both are negatively charged over a wide pH range as well as absorb over a broad UV range so that they can be analyzed simultaneously by capillary electrophoresis. In this paper, different separation strategies for the analysis of nitrite and nitrate by capillary electrophoresis with direct UV abso rbance detection are presented
Tárgyszavak:	Orvostudományok Elméleti orvostudományok idegen nyelvű folyóiratközlemény hazai lapban folyóiratcikk capillary electrophoresis nitrite nitrate, analysis
Megjelenés:	Hungarian Journal of Industrial Chemistry. - 53 : 2 (2025), p. 73-78. -
További szerzők:	Hogyor Kinga Járvás Gábor (1982-) (vegyészmérnök) Guttman András (1954-) (vegyészmérnök)
Pályázati támogatás:	PTP2025 Egyéb NKFIH ADVANCED-150780 Egyéb
Internet cím:	Szerző által megadott URL DOI Intézményi repozitóriumban (DEA) tárolt változat
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001-es BibID:	BIBFORM116213
035-os BibID:	(WoS)001104988800001 (Scopus)85178183698
Első szerző:	Farsang Róbert
Cím:	Capillary Zone Electrophoresis of 8-Aminopyrene-1,3,6-trisulfonic Acid Labeled Carbohydrates with Online Electrokinetic Sample Cleanup / Farsang Robert, Hogyor Kinga, Jarvas Gabor, Guttman Andras
Dátum:	2023
ISSN:	0003-2700
Megjegyzések:	Capillary electrophoresis is one of the frequently used separation techniques for the analysis of complex carbohydrates. Since sugars lack chromophore or fluorophore groups, their capillary electrophoresis analysis usually requires tagging by a charged fluorophore. To speed up the derivatization reaction, a large excess of the labeling reagent is typically used; therefore, a purification step is necessary prior to CE analysis using the industry standard low-pH gel-buffer system. In addition to representing an extra sample preparation step with the associated labor and cost, the purification process also holds the risk of losing some of the sample components. In this paper we introduce an online electrokinetic sample cleanup process with electroosmotic flow (EOF)-assisted separation in a bare fused silica capillary using alkaline pH background electrolyte and normal polarity separation voltage. 8-Aminopyrene-1,3,6-trisulfonic acid (APTS)-labeled maltooligosaccharides were analyzed first to understand the complex effect of the downstream EOF and the counter current electromigration of the sample components including the labeling dye. The use of 150 mM caproic acid?253 mM Tris (pH 8.1) running buffer facilitated the entrance of the sample components of interest into the separation capillary, while the excess labeling reagent was excluded and, therefore, did not interfere with the detection. The alkaline caproic acid?Tris running buffer was then applied to the N-glycome analysis of human serum samples, showing excellent separation performance, and more importantly, the extra sample purification step was not required.
Tárgyszavak:	Orvostudományok Elméleti orvostudományok idegen nyelvű folyóiratközlemény külföldi lapban folyóiratcikk Capillary electrophoresis Carbohydrates Electroosmosis Labeling Polarity
Megjelenés:	Analytical Chemistry. - 95 : 45 (2023), p. 16459-16464. -
További szerzők:	Hogyor Kinga Járvás Gábor (1982-) (vegyészmérnök) Guttman András (1954-) (vegyészmérnök)
Pályázati támogatás:	DE TUDFIN Egyéb
Internet cím:	Szerző által megadott URL DOI Intézményi repozitóriumban (DEA) tárolt változat
Borító:
Saját polcon: